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  • Title: Stereocontrol in solid-phase radical reactions: radical addition to oxime ether anchored to polymer support.
    Author: Miyabe H, Konishi C, Naito T.
    Journal: Org Lett; 2000 May 18; 2(10):1443-5. PubMed ID: 10814468.
    Abstract:
    A high degree of stereocontrol in solid-phase radical reactions was achieved by using triethylborane and diethylzinc as a radical initiator at low reaction temperature. Alkyl radical addition to Oppolzer's camphorsultam derivatives of oxime ether anchored to polymer support proceeded smoothly to give the alpha-amino acid derivatives with excellent diastereoselectivities.
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