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  • Title: Synthetic studies toward phorboxazole A. stereoselective synthesis of the C(28)-C(46) side chain fragment.
    Author: Williams DR, Clark MP, Emde U, Berliner MA.
    Journal: Org Lett; 2000 Sep 21; 2(19):3023-6. PubMed ID: 10986098.
    Abstract:
    A stereoselective synthesis of the C(28)-C(46) fragment (3) of phorboxazole A is described. Key advances include an enantioselective allylation to establish the stereochemistry of the tetrahydropyran unit and a useful SmI(2)-mediated modification of the Barbier reaction of iodomethyloxazole 15 with aldehyde 14.
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