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  • Title: Lasonolide A: structural revision and synthesis of the unnatural (-)-enantiomer.
    Author: Lee E, Song HY, Kang JW, Kim DS, Jung CK, Joo JM.
    Journal: J Am Chem Soc; 2002 Jan 23; 124(3):384-5. PubMed ID: 11792202.
    Abstract:
    Total synthesis of the unnatural (-)-enantiomer of lasonolide A was achieved starting from ethyl l-malate. The two tetrahydropyranyl fragments were prepared stereoselectively via radical cyclization reactions of beta-alkoxyacrylates. The full structure of natural lasonolide A was determined unequivocally.
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