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  • Title: Synthesis of (25R)-26-hydroxycholesterol.
    Author: Williams JR, Chai D, Wright D.
    Journal: Steroids; 2002 Dec; 67(13-14):1041-4. PubMed ID: 12441189.
    Abstract:
    We describe the synthesis of (25R)-cholest-5-en-3beta,26-diol ((25R)-26-hydroxycholesterol) from diosgenin in four steps in 58% overall, yield via a modified Clemmensen reduction followed by a Barton deoxygenation reaction.
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