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  • Title: Gas-liquid chromatographic headspace method for vinyl chloride in vinegars and alcoholic beverages.
    Author: Williams DT.
    Journal: J Assoc Off Anal Chem; 1976 Jan; 59(1):30-1. PubMed ID: 1249038.
    Abstract:
    Vinyl chloride (VC) is determined in vinegars and alcoholic beverages by gas-liquid chromatographic headspace analysis. The lower limit of detection is 10 ppb and confirmation by gas chromatography-mass spectrometry, single ion monitoring at m/e 62, is possible at this level. Comparison of the headspace and the direct injection methods for the determination of VC in vinegars and alcoholic beverages showed that the results obtained by the 2 methods were not significantly different (P greater than 0.05).
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