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  • Title: A ring-closing metathesis approach toward formal total synthesis of (+)-diplodialide A.
    Author: Anand RV, Baktharaman S, Singh VK.
    Journal: J Org Chem; 2003 Apr 18; 68(8):3356-9. PubMed ID: 12688821.
    Abstract:
    An asymmetric formal total synthesis of diplodialide A 1a has been achieved starting from methyl acetoacetate 6 and (R)-3-buten-2-ol 7. The macrocyclic ring core of (+)-diplodialide A 1a was constructed, in an excellent yield, by using a ring-closing metathesis strategy.
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