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  • Title: Enantioselective total synthesis of (+)-rogioloxepane A.
    Author: Crimmins MT, DeBaillie AC.
    Journal: Org Lett; 2003 Aug 21; 5(17):3009-11. PubMed ID: 12916968.
    Abstract:
    [reactiojn: see text] The enantioselective synthesis of (+)-rogioloxepane A has been achieved in 21 steps from 1,5-hexadien-3-ol. The key steps in the synthesis are an asymmetric glycolate alkylation leading to the diene 2 and a subsequent ring-closing metathesis to construct the oxepene core.
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