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  • Title: Determination of methacrylonitrile in serum using gas chromatography and flame ionization detection.
    Author: Demby KB, White TC, Ghanayem BI.
    Journal: J Chromatogr; 1992 Aug 07; 579(1):153-7. PubMed ID: 1447342.
    Abstract:
    A gas chromatographic method is described for the quantitation of methacrylonitrile in serum. Methacrylonitrile was extracted from rat serum with diethyl ether and then quantified using a gas chromatograph equipped with a flame ionization detector and a 60-m megabore column coated with polyethylene glycol polymer. The recoveries obtained following a one-step extraction with diethyl ether varied from 60% at 3.2 micrograms/ml to 70% at 80 micrograms/ml. The coefficient of variation for the analysis ranged from 2.5% at 400 micrograms/ml to 15.0% at 3.2 micrograms/ml.
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