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  • Title: Water-protein interactions in microcrystalline crh measured by 1H-13C solid-state NMR spectroscopy.
    Author: Lesage A, Böckmann A.
    Journal: J Am Chem Soc; 2003 Nov 05; 125(44):13336-7. PubMed ID: 14583011.
    Abstract:
    Using solid-state NMR carbon-proton dipolar correlation spectroscopy, we observed hydrogen exchange on the millisecond time scale between water molecules and protein protons in a solid sample. These interactions are shown to be related to important structural features of the protein such as hydrogen-bonding or salt-bridge networks.
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