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  • Title: Transverse dephasing optimized solid-state NMR spectroscopy.
    Author: De Paëpe G, Giraud N, Lesage A, Hodgkinson P, Böckmann A, Emsley L.
    Journal: J Am Chem Soc; 2003 Nov 19; 125(46):13938-9. PubMed ID: 14611212.
    Abstract:
    It is shown how coherence lifetimes in solid-state NMR experiments can be controlled. New decoupling schemes are introduced which actively optimize dephasing times, providing increases of up to a factor of 2 with respect to the best existing schemes. The new schemes are implemented in transverse-dephasing-optimized (TDOP) NMR experiments for the disorded solid cellulose, and for a microcrystalline protein, where sensitivity improvements of up to a factor of 5 are obtained.
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