These tools will no longer be maintained as of December 31, 2024. Archived website can be found here. PubMed4Hh GitHub repository can be found here. Contact NLM Customer Service if you have questions.


Pubmed for Handhelds

PUBMED FOR HANDHELDS

Search MEDLINE/PubMed

  • Title: Direct structure determination of a multicomponent molecular crystal prepared by a solid-state grinding procedure.
    Author: Cheung EY, Kitchin SJ, Harris KD, Imai Y, Tajima N, Kuroda R.
    Journal: J Am Chem Soc; 2003 Dec 03; 125(48):14658-9. PubMed ID: 14640612.
    Abstract:
    A three-component molecular cocrystal material has been prepared by a solvent-free route involving mechanical grinding of the pure phases of the individual components. This material is not accessible from conventional solution-state crystallization procedures. Due to the fact that the grinding procedure intrinsically leads to a microcrystalline powder sample, the use of powder X-ray diffraction data is essential for structure determination. This work emphasizes the scope and utility of ab initio structure solution directly from powder X-ray diffraction data for carrying out structural characterization of new materials prepared via the solid-state grinding route, leading to the opportunity to establish structure-property relationships for such materials.
    [Abstract] [Full Text] [Related] [New Search]