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  • Title: Synthesis of the cyclobutanone core of solanoeclepin A intramolecular allene butenolide photocycloaddition.
    Author: Hue BT, Dijkink J, Kuiper S, Larson KK, Guziec FS, Goubitz K, Fraanje J, Schenk H, van Maarseveen JH, Hiemstra H.
    Journal: Org Biomol Chem; 2003 Dec 21; 1(24):4364-6. PubMed ID: 14685306.
    Abstract:
    The compact tricyclic substructure of solanoeclepin A containing the cyclobutanone ring was prepared by using as the key step a highly regioselective intramolecular [2 + 2]-photocycloaddition reaction between one of the [small pi]-bonds of an allene and the CC double bond of a butenolide.
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