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  • Title: Solid-phase tandem radical addition-cyclization reaction: triethylborane-induced reaction of oxime ethers anchored to polymer support.
    Author: Miyabe H, Tanaka H, Naito T.
    Journal: Chem Pharm Bull (Tokyo); 2004 Jul; 52(7):842-7. PubMed ID: 15256705.
    Abstract:
    Tandem radical addition-cyclization of oxime ethers anchored to polymer support was studied. The reaction of oxime ethers with stannyl radical proceeded effectively by the use of triethylborane as a radical initiator. The alkyl radical addition-cyclization reactions of oxime ether connected with alpha,beta-unsaturated carbonyl group proceeded under iodine atom-transfer reaction conditions to give the functionalized azacycles via two carbon-carbon bonds-forming process.
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