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  • Title: Toward the total synthesis of phorboxazole B: an efficient synthesis of the C20-C46 segment.
    Author: Li DR, Sun CY, Su C, Lin GQ, Zhou WS.
    Journal: Org Lett; 2004 Nov 11; 6(23):4261-4. PubMed ID: 15524458.
    Abstract:
    An efficient synthesis of the C20-C46 segment of phorboxazole B is described. The key steps involved Hg(OAc)(2)/I(2)-induced cyclization to construct the cis-tetrahydropyran moiety, the coupling of the metalated 2-methyloxazole 7 with lactone 6, and Julia olefination to furnish the conjugated diene moiety.
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