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  • Title: Synthesis of homoleptic barium alkoxides and aryloxides and their reactions with Al(CH(3))(3): a convenient route to heterometallic species.
    Author: Utko J, Szafert S, Jerzykiewicz LB, Sobota P.
    Journal: Inorg Chem; 2005 Jul 25; 44(15):5194-6. PubMed ID: 16022512.
    Abstract:
    Reactions of metallic Ba with benzofuranol (dbbfoH) or diethylene glycol give homoleptic and homonuclear complexes Ba(dbbfo)(2)(dbbfoH)(2).3dbbfoH and Ba{O(CH(2)CH(2)O)(2)}{O(CH(2)CH(2)OH)(2)}(2) (60-89%). Both compounds and formerly described Ba{O(CH(2)CH(2)O)(2)Me}(2) react with Al(CH(3))(3) to yield trinuclear heterobimetallic low-coordinated barium compounds with structure and geometry depending on the reaction stoichiometry and crystallization procedure.
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