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  • Title: Solvolytic routes to new nonabismuth hydroxy- and alkoxy-oxo complexes: synthesis, characterization and solid-state structures of novel nonabismuth polyoxo cations Bi9(mu3-O)8(mu3-OR)6 5+ (R = H, Et).
    Author: Thurston JH, Swenson DC, Messerle L.
    Journal: Chem Commun (Camb); 2005 Sep 07; (33):4228-30. PubMed ID: 16100612.
    Abstract:
    Base hydrolysis of BiO(ClO4) yields ClO4- salts of the novel nonabismuth polyoxo cation Bi9(mu3-O)8(mu3-OH)6(5+); ethanolysis converts to the ethoxide Bi9(mu3-O)8(mu3-OEt)6(5+).
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