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  • Title: Determination of Zy 17617B in plasma by solid-phase extraction and liquid chromatography with automated pre-column exchange.
    Author: Chollet D, Salanon M.
    Journal: J Chromatogr; 1992 Feb 28; 593(1-2):73-8. PubMed ID: 1639914.
    Abstract:
    An automated chromatographic system, combining solid-phase extraction and automated pre-column exchange, is described for the routine determination of Zy 17617B at the pmol/ml level in human plasma. The sample extraction and elution onto the analytical column were performed automatically and concomitantly using a conventional liquid chromatographic apparatus equipped with a Merck OSP-2 on-line sample preparator. Validation data demonstrate the reliability of the method.
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