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  • Title: Synthesis, characterization, and X-ray crystal structure of a gallium monohydroxide and a hetero-bimetallic gallium zirconium oxide.
    Author: Singh S, Jancik V, Roesky HW, Herbst-Irmer R.
    Journal: Inorg Chem; 2006 Feb 06; 45(3):949-51. PubMed ID: 16441096.
    Abstract:
    A monomeric hydroxide of gallium, LGa(Me)OH, containing terminal hydroxide and methyl groups was prepared by the hydrolysis of LGa(Me)Cl in the presence of N-heterocyclic carbene and water [L = HC{(CMe)(2,6-i-Pr2C6H3N)}2] in high yield and in a pure form. LGa(Me)OH was used as a synthon to assemble the first hetero-bimetallic compound with a Ga-O-Zr core, [(LGaMe)(Cp2ZrMe)](mu-O).
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