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  • Title: Synthesis of glycosyl phosphates from 1,2-orthoesters and application to in situ glycosylation reactions.
    Author: Ravidà A, Liu X, Kovacs L, Seeberger PH.
    Journal: Org Lett; 2006 Apr 27; 8(9):1815-8. PubMed ID: 16623558.
    Abstract:
    [reaction: see text] A series of glycosyl phosphates were prepared in high yield by treatment of the corresponding 1,2-orthoesters with dibutyl phosphate. Glycosyl phosphates are efficient glycosylating agents even when used in crude form or when generated in situ. The immunodominant epitope trirhamnoside of group B Streptococcus was prepared to demonstrate the synthetic utility of the method.
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