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  • Title: First total synthesis of (+/-)-3-aza-11-oxa-1,3,5(10)-trieno steroids.
    Author: Oumzil K, Ibrahim-Ouali M, Santelli M.
    Journal: Steroids; 2006 Oct; 71(10):886-94. PubMed ID: 16834992.
    Abstract:
    We set out to describe a new and versatile method for preparing 3-aza-11-oxa-1,3,5(10)-trieno steroids via an intramolecular Diels-Alder cycloaddition of o-quinodimethanes as the key step. The characteristic 1H and 13C NMR spectroscopic features of the synthesized compounds are reported.
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