These tools will no longer be maintained as of December 31, 2024. Archived website can be found here. PubMed4Hh GitHub repository can be found here. Contact NLM Customer Service if you have questions.


Pubmed for Handhelds

PUBMED FOR HANDHELDS

Search MEDLINE/PubMed

  • Title: The effect of five silane coupling agents on the bond strength of a luting cement to a silica-coated titanium.
    Author: Matinlinna JP, Lassila LV, Vallittu PK.
    Journal: Dent Mater; 2007 Sep; 23(9):1173-80. PubMed ID: 17126393.
    Abstract:
    OBJECTIVES: The adhesive performance of five silane coupling agents in adhering resin composite cement (3M ESPE) to silica-coated titanium was evaluated. Titanium was tribochemically silica-coated by using the Rocatec system. METHODS: Two volume percent solutions of 3-acryloyloxypropyltrimethoxysilane (Toray Dow Corning Silicone), N-[3-(trimethoxysilyl)propylethylenediamine] (Dow Corning), 3-mercaptopropyltrimethoxysilane (Toray Dow Corning Silicone) and bis-[3-(triethoxysilyl)propyl]polysulfide (Dow Corning) were prepared in 95 vol.% acidified ethanol and allowed to activate (hydrolyze). A pre-activated ca. 2 vol.% 3-methacryloyloxypropyltrimethoxysilane (ESPE Sil) was used as a control. The silanes were applied onto silica-coated titanium slides. Chemical activation reactions of the silanes were monitored by Fourier transform infrared spectrometry (Perkin-Elmer Spectrum One). RelyX ARC (3M ESPE) resin composite cement stubs were applied and photo-polymerized onto silica-coated titanium. The specimens were thermo-cycled (6000 cycles, 5-55 degrees C). RESULTS: Statistical analysis (ANOVA) showed that the highest shear bond strength (n=8 per group) value after thermocycling, 14.8 MPa (S.D. 3.8 MPa), was obtained with 2.0 vol.% 3-acryloyloxypropyltrimethoxysilane. Silanization and results with 3-methacryloyloxypropyltrimethoxysilane (control, ESPE Sil) did not statistically differ from 3-acryloyloxypropyltrimethoxysilane, 14.2 MPa (S.D. 5.8). The lowest shear bond strength was 7.5 (S.D. 1.9) MPa for N-[3-(trimethoxysilyl)propylethylenediamine] and 7.5 (S.D. 2.5) MPa for bis-[3-(triethoxysilyl)propyl]polysulfide. Both the type of silane (p<0.001) and storage conditions affected significantly the shear bond strength values (p<0.001). All silanes became activated according to the infrared spectroscopic analysis. SIGNIFICANCE: Silanization with 3-acryloyloxypropyltrimethoxysilane or 3-mercaptopropyltrimethoxysilane might offer an alternative for bonding a luting cement to silica-coated titanium.
    [Abstract] [Full Text] [Related] [New Search]