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  • Title: Application of a hybrid pixel detector to powder diffraction.
    Author: Basolo S, Bérar JF, Boudet N, Breugnon P, Caillot B, Clemens JC, Delpierre P, Dinkespiler B, Hustache S, Koudobine I, Meessen Ch, Menouni M, Mouget C, Palancher H, Pangaud P, Potheau R, Vigeolas E.
    Journal: J Synchrotron Radiat; 2007 Jan; 14(Pt 1):151-7. PubMed ID: 17211083.
    Abstract:
    Results obtained using a hybrid pixel photon-counting detector in powder diffraction experiments are presented. The detector works at room temperature and its dynamic response ranges from 0.01 photons pixel(-1) s(-1) up to 10(6) photons pixel(-1) s(-1). The pixel sizes are 0.33 mm x 0.33 mm for a total area of 68 mm x 68 mm. On recording high-resolution diffraction patterns of powders, a reduction of the experimental time by more than a factor of 20 is obtained without loss of data quality. The example of an X-zeolite shows that such detectors can be used for very demanding anomalous experiments. In situ experiments of quenching liquid oxides show that frames of 0.01 s can be achieved for studying such processes.
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