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  • Title: Synthesis and absolute structure of manzacidin B.
    Author: Shinada T, Ikebe E, Oe K, Namba K, Kawasaki M, Ohfune Y.
    Journal: Org Lett; 2007 Apr 26; 9(9):1765-7. PubMed ID: 17411060.
    Abstract:
    [reaction: see text] Four possible stereoisomers of manzacidin B were synthesized using stereochemically defined synthetic routes via the azide 7 and oxazoline 11 starting with the (R)-alpha-methyl Garner aldehyde 5. Comparisons of the spectroscopic data of the synthetic isomers 4a-d with those of the natural manzacidin B revised the proposed structure 3 to (4S,5S,6R)-4d.
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