These tools will no longer be maintained as of December 31, 2024. Archived website can be found here. PubMed4Hh GitHub repository can be found here. Contact NLM Customer Service if you have questions.


Pubmed for Handhelds

PUBMED FOR HANDHELDS

Search MEDLINE/PubMed

  • Title: Organic solvents-free technique for determining sulfadimethoxine and its metabolites in chicken meat.
    Author: Furusawa N.
    Journal: J Chromatogr A; 2007 Nov 16; 1172(1):92-5. PubMed ID: 17936765.
    Abstract:
    A quick and cost-effective technique of sample preparation followed by a reversed-phase high performance liquid chromatography under "organic solvent-free" (=100% aqueous) conditions for the simultaneous quantifying of sulfadimethoxine (SDM) and its metabolites, 6-hydroxy SDM (6-OH) and N(4)-acetyl SDM (N(4)-Ac), in chicken muscle is presented. Analysis by HPLC with photo-diode array detector was performed using a short C1 column with an isocratic 0.04 mol/l citric acid mobile phase. The method was validated by the analyses of spiked chicken muscle samples, resulting recoveries (> or =84%; relative standard deviations < or =6%), analytical total time (<1/2 h/sample, where a batch of 12 samples in 4 h), and limits of quantitation (< or =0.1 microg/g). The decision limits and detection capability were 0.019-0.106 and 0.054-0.112 microg/g, respectively. No organic solvents were used at all.
    [Abstract] [Full Text] [Related] [New Search]