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  • Title: [Determination of chloropromazine residues in animals kidney and urine using LC-MS/MS method].
    Author: Rodziewicz L, Zawadzka I.
    Journal: Rocz Panstw Zakl Hig; 2007; 58(3):503-8. PubMed ID: 18246654.
    Abstract:
    Chloropromazina (CP) is subjected to monitoring food animals products, with a minimum required performance limit (MPRL) set 5.0 microg/kg. Homogenized kidney and urine were extracted with acetonitrile. CP- d3 was used as internal standard. LC separation was done on Luna C18 150 x 2 mm, 5 microm column in mobile phase acetonitrile-acetic acid. CP was determination by LC-ESI-MS/MS negative mode. The method was validation according to the criteria of Decision Commission No 2002/657/EC. Recoveries for the level 5.0 ng/g were in the range 84-102%. The limit of decision (CCalpha) and detection capability (CCbeta) CP in kidney were 1.19; 2.87 ng/g and urine 1.08; 2.61 ng/g.
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