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  • Title: Mild and efficient Re(VII)-catalyzed synthesis of 1,1-dihydroperoxides.
    Author: Ghorai P, Dussault PH.
    Journal: Org Lett; 2008 Oct 16; 10(20):4577-9. PubMed ID: 18783232.
    Abstract:
    Re2O7 in CH3CN is a remarkably efficient and mild catalyst for the peroxyacetalization of ketones, aldehydes, or acetals by H2O2 to generate 1,1-dihydroperoxides. Me3SiOReO3 and methyl rhenium trioxide (MTO) are also effective catalysts under these reaction conditions.
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