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  • Title: Total synthesis of azumamide E and sugar amino acid-containing analogue.
    Author: Chandrasekhar S, Rao CL, Seenaiah M, Naresh P, Jagadeesh B, Manjeera D, Sarkar A, Bhadra MP.
    Journal: J Org Chem; 2009 Jan 02; 74(1):401-4. PubMed ID: 19053574.
    Abstract:
    An efficient and practical total synthesis of marine cyclic tetrapeptide, natural product azumamide E (1) is achieved via high-yielding reactions. The strategy also allowed us to synthesize the azumamide E-SAA (sugar amino acid) analogue (2), whose solution-phase NMR and biological activity studies were also carried out.
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