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  • Title: Spectroscopic study and structure of (E)-2-[(2-chlorobenzylimino)methyl]methoxyphenol.
    Author: Unver H, Yildiz M, Ozay H, Durlu TN.
    Journal: Spectrochim Acta A Mol Biomol Spectrosc; 2009 Dec; 74(5):1095-9. PubMed ID: 19879183.
    Abstract:
    (E)-2-[(2-chlorobenzylimino)methyl]methoxyphenol has been synthesized from the reaction of 2-hydroxy-3-methoxy-1-benzaldehyde(o-vanillin) with 2-chlorobenzylamine. The title compound has been characterized by using elemental analysis, FT-IR, (1)H NMR, (13)C NMR and UV-vis spectroscopic techniques. The crystal structure of the title compound has also been examined cyrstallographically. It crystallizes in the orthorhombic space group Pbca with unit cell parameters: a = 7.208(1) A, b = 13.726(2) A, c = 27.858(4) A, V = 2756.0(1) A(3), D(c) = 1.18 g cm(-3) and Z = 8. The crystal structure was solved by direct methods and refined by full-matrix least squares to a find R = 0.046 for 2773 observed reflections.
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