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  • Title: Palladium-catalyzed preparation of Weinreb amides from boronic acids and N-methyl-N-methoxycarbamoyl chloride.
    Author: Krishnamoorthy R, Lam SQ, Manley CM, Herr RJ.
    Journal: J Org Chem; 2010 Feb 19; 75(4):1251-8. PubMed ID: 20088577.
    Abstract:
    A simple protocol for the synthesis of Weinreb benzamides and alpha,beta-unsaturated Weinreb amides through a palladium-catalyzed cross-coupling reaction between organoboronic acids and N-methoxy-N-methylcarbamoyl chloride has been developed. The method is also applicable to the use of potassium organotrifluoroborates.
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