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  • Title: Solid-phase de novo synthesis of a (+/-)-2-deoxy-glycoside.
    Author: Lucchesi C, Arboré A, Pascual S, Fontaine L, Maignan C, Dujardin G.
    Journal: Carbohydr Res; 2010 Apr 19; 345(6):844-9. PubMed ID: 20171610.
    Abstract:
    The solid-phase synthesis of methyl 2-deoxy-3-O-benzyl-D,L-arabino-hexopyranoside was achieved in a six-step sequence via a de novo strategy based on the hetero-Diels-Alder reaction of a vinyl ether supported on an azalactone-functionalized polystyrene resin, followed by the functional modification of the heteroadduct and the final release of the methyl glycoside by acidic solvolysis.
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