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  • Title: Palladium-catalyzed cyclocarbonylation of arynes with methyl allyl carbonates: selective synthesis of 1H-inden-1-ones.
    Author: Pi SF, Yang XH, Huang XC, Liang Y, Yang GN, Zhang XH, Li JH.
    Journal: J Org Chem; 2010 May 21; 75(10):3484-7. PubMed ID: 20373751.
    Abstract:
    A selective protocol for the synthesis of 2-methylene-3-substituted-2,3-dihydro-1H-inden-1-ones and 2-benzylidene-2,3-dihydro-1H-inden-1-ones has been developed via palladium-catalyzed cyclocarbonylation reactions of arynes with allyl carbonates and carbon monooxide (CO). It is noteworthy that the selectivity of this new route is depended on both substrates and ligands.
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