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  • Title: Solid-phase extraction of fluoxetine and norfluoxetine from serum with gas chromatography-electron-capture detection.
    Author: Dixit V, Nguyen H, Dixit VM.
    Journal: J Chromatogr; 1991 Feb 15; 563(2):379-84. PubMed ID: 2056002.
    Abstract:
    A rapid, selective, and sensitive method is described for the purification and analysis of fluoxetine and norfluoxetine using a solid-phase extraction column and gas chromatography-electron-capture detection. Linear quantitative response curves for fluoxetine and norfluoxetine are generated over a concentration range of 20-200 ng/ml. Overall extraction efficiency of the extraction procedure is found to be greater than 90% and greater than 75% with correlation coefficients of 0.997 and 0.993 for fluoxetine and norfluoxetine, respectively.
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