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  • Title: Benzoyl peroxide (BPO)-promoted oxidative trifluoromethylation of tertiary amines with trimethyl(trifluoromethyl)silane.
    Author: Chu L, Qing FL.
    Journal: Chem Commun (Camb); 2010 Sep 14; 46(34):6285-7. PubMed ID: 20694243.
    Abstract:
    The benzoyl peroxide (BPO)-promoted oxidative functionalization of tertiary amines under transition-metal-free reaction conditions was developed. Various 1-trifluoromethylated tetrahydroisoquinoline derivatives were prepared by employing this method. It constitutes the first example of direct trifluoromethylation of tertiary amines.
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