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  • Title: Solvent-free microwave-assisted multi-component reaction for preparation of 2-amino-1-aryl-2-(cyclohex-1-enyl)ethanones as precursors of pseudoephedrine analogues.
    Author: Ma LJ, Inokuchi T.
    Journal: Chem Commun (Camb); 2010 Oct 07; 46(37):7037-9. PubMed ID: 20737087.
    Abstract:
    Microwave irradiation of chloroacetylarenes and enamines induced an aza-Darzens reaction followed by rearrangement of the aziridinium intermediate to give (2-amino-3-alkenoyl)arenes that were reduced selectively to syn-beta-aminoalcohols as pseudo-ephedrine analogues.
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