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  • Title: Synthesis of 12-oxa, 12-aza and 12-thia cholanetriols.
    Author: Ibrahim-Ouali M, Hamze K, Rocheblave L.
    Journal: Steroids; 2011 Feb; 76(3):324-30. PubMed ID: 21163283.
    Abstract:
    An efficient synthesis of 12-hetero steroids was achieved via a Baeyer-Villiger oxidation and a photolysis as the key steps. We set out to describe in this paper the first synthesis of 12-aza steroids. The characteristic (1)H and (13)C NMR spectroscopic features of the synthesized compounds are reported.
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