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  • Title: The asymmetric Maitland-Japp reaction and its application to the construction of the C1-C19 bis-pyran unit of phorboxazole B.
    Author: Clarke PA, Santos S, Mistry N, Burroughs L, Humphries AC.
    Journal: Org Lett; 2011 Feb 18; 13(4):624-7. PubMed ID: 21247215.
    Abstract:
    The synthesis of the C1-C19 bis-pyran unit of phorboxazole B has been achieved. The key pyran rings were constructed by means of an asymmetric Maitland-Japp reaction and a second Maitland-Japp resolution/cyclization reaction. The longest linear sequence was 14 steps, and the C1-C19 bis-pyran unit was formed in an impressive 10.4% yield.
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