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  • Title: One-pot asymmetric synthesis of γ-nitroaldehydes from aldehydes and nitroalkanes through a catalytic tandem reaction using an amino acid lithium salt.
    Author: Yoshida M, Kitamikado N, Ikehara H, Hara S.
    Journal: J Org Chem; 2011 Apr 01; 76(7):2305-9. PubMed ID: 21388203.
    Abstract:
    One-pot asymmetric synthesis of γ-nitroaldehydes from aldehydes and nitroalkanes was achieved by a catalytic tandem reaction using a primary amino acid lithium salt, O-tert-butyldiphenylsilyl l-tyrosine lithium salt, as a catalyst. Various aryl, alkenyl, and alkyl aldehydes were converted into γ-nitroaldehydes via in situ generation of nitroalkenes.
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