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Title: One-pot hydrothermal synthesis of uniform β-MnO2 nanorods for nitrite sensing. Author: Feng JJ, Zhang PP, Wang AJ, Zhang Y, Dong WJ, Chen JR. Journal: J Colloid Interface Sci; 2011 Jul 01; 359(1):1-8. PubMed ID: 21507413. Abstract: A simple hydrothermal method was developed for the synthesis of uniform single-crystal β-MnO(2) nanorods only using potassium permanganate and sodium nitrite in acidic solution, without any seed or template. The as-prepared β-MnO(2) nanorods have the average diameter of 300±20 nm and a length up to 1.2±0.2 μm. Moreover, the effects of pH, temperature, and reactant molar ratios on the morphology of the final product were studied in detail. In addition, the catalytic ability of the as-prepared β-MnO(2) nanorods was tested for the electrooxidation of nitrite. The resulting sensor showed a wide linear range from 0.29 μM to 26.09 mM (R=0.9986), high sensitivity (1.21 μA mM(-1), S/N=3), low detection limit (0.29 μM), and fast response (less than 5 s).[Abstract] [Full Text] [Related] [New Search]