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  • Title: Synthesis and characterization of iron(II) and ruthenium(II) hydrido hydrazine complexes.
    Author: Field LD, Li HL, Dalgarno SJ, Jensen P, McIntosh RD.
    Journal: Inorg Chem; 2011 Jun 20; 50(12):5468-76. PubMed ID: 21618998.
    Abstract:
    Treatment of trans-[MHCl(dmpe)(2)] (M = Fe, Ru) with hydrazine afforded the hydrido hydrazine complexes cis- and trans-[MH(N(2)H(4))(dmpe)(2)](+) which have been characterized by NMR spectroscopy ((1)H, (31)P, and (15)N). Both cis and trans isomers of the Fe complex and the trans isomer of the Ru complex were characterized by X-ray crystallography. Reactions with acid and base afforded a range of N(2)H(x) complexes, including several unstable hydrido hydrazido complexes.
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