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  • Title: Complete assignment of NMR data of 22 phenyl-1H-pyrazoles' derivatives.
    Author: de Oliveira AL, Alves de Oliveira CH, Mairink LM, Pazini F, Menegatti R, Lião LM.
    Journal: Magn Reson Chem; 2011 Aug; 49(8):537-42. PubMed ID: 21761453.
    Abstract:
    Complete assignment of (1)H and (13)C NMR chemical shifts and J((1)H/(1)H and (1)H/(19)F) coupling constants for 22 1-phenyl-1H-pyrazoles' derivates were performed using the concerted application of (1)H 1D and (1)H, (13)C 2D gs-HSQC and gs-HMBC experiments. All 1-phenyl-1H-pyrazoles' derivatives were synthesized as described by Finar and co-workers. The formylated 1-phenyl-1H-pyrazoles' derivatives were performed under Duff's conditions.
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