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  • Title: A novel and highly stereoselective synthesis of 2-substituted perhydrofuro[2,3-b]pyran derivatives.
    Author: Ma X, Tian Q, Tang Q, Zhao J, Shao H.
    Journal: Org Lett; 2011 Aug 19; 13(16):4276-9. PubMed ID: 21774487.
    Abstract:
    An effective and facile method for the synthesis of 2-substituted perhydrofuro[2,3-b]pyran derivatives is described. The cyclization of 2-C-aldehydo-2-deoxy-D-thioglucoside in the presence of N-iodosuccinimide (NIS) is highly stereoselective. 2-Substituted cyclization products were obtained in good to excellent yields.
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