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  • Title: Synthesis and vibrational spectroscopic analysis of some Hofmann type clathrates.
    Author: Parlak C, Şenyel M.
    Journal: Spectrochim Acta A Mol Biomol Spectrosc; 2011 Nov; 82(1):383-8. PubMed ID: 21820947.
    Abstract:
    New Hofmann type clathrates in the form of M(pp)(2)Ni(CN)(4)·2G (where pp = 1-phenylpiperazine, G = 1,4-dioxane and M = Ni, Co or Cd) have been prepared in powder form and their FT-IR and FT-Raman spectra are reported. The results suggest that the present compounds are similar in structure to the Hofmann type clathrates and their structures consist of conjugated polymeric layers of |M-Ni(CN)(4)|(∞) with the pp bound to the metal (M) atom.
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