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Title: Synthesis and structural analysis of a highly curved buckybowl containing corannulene and sumanene fragments. Author: Wu TC, Hsin HJ, Kuo MY, Li CH, Wu YT. Journal: J Am Chem Soc; 2011 Oct 19; 133(41):16319-21. PubMed ID: 21932840. Abstract: Buckybowls 7, 9, and 10 were prepared from benzo[k]fluoranthene 6 and fluoranthene 8 using straightforward procedures involving key palladium-catalyzed cyclization reactions. The structures of bowl-shaped molecules 7 and 10 were determined by using X-ray crystallographic methods. The observed p-orbital axis vector (POAV) angle of 7 was found to be 12.8°.[Abstract] [Full Text] [Related] [New Search]