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  • Title: Asymmetric aziridination of cyclic enones using chiral diamine catalysts and its application to the total synthesis of (-)-agelastatin A.
    Author: Menjo Y, Hamajima A, Sasaki N, Hamada Y.
    Journal: Org Lett; 2011 Nov 04; 13(21):5744-7. PubMed ID: 21966984.
    Abstract:
    The asymmetric aziridination of cyclic enones with N-tosyloxycarbamates, using N-neopentyl 1,2-diphenylethylenediamine as a catalyst, and its application to the formal total synthesis of (-)-agelastatin A, using a one-pot silylation-selenylation procedure and the regioselective aziridine-opening by an azide anion as key steps, are described.
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