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  • Title: Introduction of bridging and pendant organic groups into mesoporous alumina materials.
    Author: Grant SM, Woods SM, Gericke A, Jaroniec M.
    Journal: ACS Appl Mater Interfaces; 2011 Nov; 3(11):4480-6. PubMed ID: 21988174.
    Abstract:
    Incorporation of organic functionalities into soft-templated mesoporous alumina was performed via organosilane-assisted evaporation induced self-assembly using aluminum alkoxide precursors and block copolymer templates. This strategy permits one to obtain mesoporous alumina-based materials with tailorable adsorption, surface and structural properties. Isocyanurate, ethane, mercaptopropyl, and ureidopropyl-functionalized mesoporous alumina materials were synthesized with relatively high surface area and large pore volume with uniform and wormhole-like mesopores. The presence of organosilyl groups within these hybrid materials was confirmed by IR or Raman spectroscopy and their concentration was determined by elemental analysis.
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