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  • Title: Application of central composite face-centered design and response surface methodology for the optimization of electro-Fenton decolorization of Azure B dye.
    Author: Rosales E, Sanromán MA, Pazos M.
    Journal: Environ Sci Pollut Res Int; 2012 Jun; 19(5):1738-46. PubMed ID: 22161116.
    Abstract:
    PURPOSE: The aim of this work was to improve the ability of electro-Fenton technique for the remediation of wastewater contaminated with synthetic dyes using a model azo dye such as Azure B. METHODS: Batch experiments were conducted to study the effects of main parameters, such as dye concentration, electrode surface area, treatment time, and voltage. In this study, central composite face-centered experimental design matrix and response surface methodology were applied to design the experiments and evaluate the interactive effects of the four studied parameters. A total of 30 experimental runs were set, and the kinetic data were analyzed using first- and second-order models. RESULTS: The experimental data fitted to the empirical second-order model of a suitable degree for the maximum decolorization of Azure B by electro-Fenton treatment. ANOVA analysis showed high coefficient of determination value (R(2) = 0.9835) and reasonable second-order regression prediction. Pareto analysis suggests that the variables, time, and voltage produce the largest effect on the decolorization rate. CONCLUSION: Optimum conditions suggested by the second-order polynomial regression model for attaining maximum decolorization were dye concentration 4.83 mg/L, electrode surface area 15 cm(2), voltage 14.19 V, and treatment time of 34.58 min.
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