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  • Title: Preparation and chiral separation of a novel immobilized cellulose-based chiral stationary phase in high-performance liquid chromatography.
    Author: Peng GM, Wu SQ, Fang ZL, Zhang WG, Zhang ZB, Fan J, Zheng SR, Wu SS, Ng SC.
    Journal: J Chromatogr Sci; 2012 Jul; 50(6):516-22. PubMed ID: 22523189.
    Abstract:
    The chiral selector 6-azido-2, 3-di(p-chlorophenylcarbamoylated) cellulose was synthesized and further chemically immobilized onto 5-μm amino functionalized spherical porous silica gel. It was used as chiral stationary phase in high-performance liquid chromatography. Thirty racemates were successfully separated into enantiomers in either normal phase mode or reversed-phase mode. Good reproducibility and stability of the chiral stationary phase have been demonstrated.
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