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  • Title: Synthesis, growth, spectral and thermal properties of a new organic crystal: 2-carboxypyridin-1-ium trichloroacetate.
    Author: Gowri S, Anitha K, Suresh A, Uma Devi T, Selvanayagam S, Sajan D, Chandramohan A, Lawrence N.
    Journal: Spectrochim Acta A Mol Biomol Spectrosc; 2012 Sep; 95():73-9. PubMed ID: 22613126.
    Abstract:
    A novel organic optical material complex of 2-carboxypyridin-1-ium trichloroacetate has been synthesized and crystals were grown from aqueous solution employing the technique of controlled evaporation. The crystal structure has been determined using single crystal X-ray diffraction studies. The single crystals were successfully grown by the slow evaporation method with dimensions 12 × 8 × 3 mm(3). FT IR spectral investigation has been carried out to identify the various functional groups present in the grown crystal. Molecular structure was confirmed by NMR spectral analysis. Melting point was found using thermal measurements.
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