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  • Title: Gas chromatographic determination of systemic fungicide tricyclazole in soil and water.
    Author: Xiao YX, Fan DF, Chen HX.
    Journal: J Assoc Off Anal Chem; 1990; 73(5):761-3. PubMed ID: 2273001.
    Abstract:
    A method is described for determination of tricyclazole residues in soil and water. Tricyclazole is extracted from soil by refluxing with ethyl acetate-acetone (80 + 20 v/v) and from water by partitioning into dichloromethane. The soil extract is purified by coagulation. The compound is detected and measured by gas chromatography using a flame photometer operated in the sulfur mode. Detection limits are 8 ppb for soil and 0.8 ppb for water. Recoveries for control samples fortified with tricyclazole at 0.1-5.0 ppm averaged 97.1% for soil and 108.1% for water.
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