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Title: Cooperative effect of polyethylene glycol and lignin on SiO2 microsphere production from rice husks. Author: Lin L, Zhai SR, Xiao ZY, Liu N, Song Y, Zhai B, An QD. Journal: Bioresour Technol; 2012 Dec; 125():172-4. PubMed ID: 23026330. Abstract: A simple method to the preparation of SiO(2) microspheres from rice husks (RH) was developed. The rice husks were extracted with 2M NaOH solution to obtain a extract contained silica and lignin, and silica spheres were obtained after addition of distilled water, ethanol, 1M H(2)SO(4) and PEG (W(silica):W(PEG)=2:1) to the extract in a controllable sol-gel process and calcination at 550°C. The optimum synthesis conditions were, adjustment of the extract to pH 3, a volume ratio of 1:1:2 of ethanol, water, and extract, respectively and a silica to polyethylene glycol weight ratio of 2:1. The SiO(2) microspheres produced under these conditions exhibited a relatively uniform particle size distribution around 500 nm as determined by LPSA, which indicated a cooperative function of added PEG and extracted lignin towards the formation of SiO(2) microspheres.[Abstract] [Full Text] [Related] [New Search]